山东LECO分析仪

Procedure - Solid Samples

Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.

Clean the upper and lower electrode manually, or, if applicable, remove the crucible and press the analyze button to clean with the automatic cleaner

Add approximately 0.05 g of *** Graphite Powder to a *** Graphite Crucible.

Firmly place the crucible on the lower electrode tip or appropriate autoloader position.

Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically

Procedure - Solid Samples

Determine the instrument blank.

Repeat steps 2b through 2g a minimum of three times.

Set the blank following the procedure outlined in the operator's instruction manual.

Instrument calibration/drift correction.

Login a minimum of 3 Standard replicates.

Weigh approximately *** grams of a calibration/drift standard, enter the mass and standard identification into appropriate replicate fields.

Note: LECO Reference Materia***o not require preparation.See preparation statement on the reference material certificate.

山东美国LECO分析仪哪家好***电极炉头设计，提高脉冲炉热交换效率。

Procedure – Powder/Chip Samples

Instrument calibration/drift correction.

Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.

Place the Nickel Capsule containing the sample into the open port at the top of the loading head.

Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.

Clean the upper and lower electrode either manually or remove the crucible and press the analyze button to clean with an automatic cleaner if applicable.

Sample Preparation

Sampling and sample preparation of refractory metals such as titanium and zirconium is somewhat different from that of steel. Unlike steel samples, hydrogen is not as mobile in this group of materials; therefore, storage in liquid nitrogen or dry ice is not required. However, it is important to keep the sample cool when cutting or sectioning. Sample preparation for oxygen and nitrogen determination has beendifferent from that of hydrogen determination.

通用下电极坩埚支座，容纳各种坩埚使用。

Instrument Highlights and Features

Features and Benefits

LED light ring illuminates the furnace area

Choice of either argon or helium carrier gas

Novel electrode design increases heat transfer efficiency for increased stability

Non-touch interface systems are also available

User-friendly brand software

High-Performance Detector Design

Thermostatic construction provides increased protection from ambient temperature fluctuations

Optimized emitter control and detection circuitryimproves the IR cell lifetime and long-term stability,

resulting in superior accuracy and precision

Infrared detection for the determination of oxygen, thermoconductivity detection for the determination

of nitrogen

采用三个**的红外器检测氧含量，同时检测CO和CO2，然后在转化为CO2集中检测。北京专业元素分析仪供应商

Cornerstone氢氧氮分析软件同时支持***的书记文档格式和可变的报告格式。山东LECO分析仪

Summary

The determination of the amount of oxygen, nitrogen, and hydrogen in iron, steel, nickel-, and cobalt-base alloys represents some of the most important quality metrics for these materials. Oxygen is used to create steel from pig iron by removing excess carbon. Oxygen content must be controlled to limit the amount of carbon monoxide that can be formed during solidification which may cause excessive porosity. Nitrogen is considered both an impurity as well as an important alloying agent. Itcan be present as a nitride or interstitially in its gaseous form. Increased nitrogen content is known to increase yield and tensile strength, thus decreasing ductility and formability. Excessive levels may evolve during solidification thus increasing porosity. High hydrogen content is the primary cause of embrittlement, blistering and flaking due to its high

mobility through the lattice and provides no potential alloying benefits. The ONH836 utilizes a high-power

electrode furnace to quickly and efficiently release the target gases from within the sample, which allows

for a very rapid simultaneous determination of oxygen, nitrogen, and hydrogen.

山东LECO分析仪

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