浙江LECO氧氮氢分析仪采购

736 Series: Oxygen/Nitrogen by Inert Gas Fusion

The 736 family of Elemental Analyzers is designed for routine measurement of oxygen and nitrogen content of

inorganic materials, ferrous and nonferrous alloys, andrefractory materials using the inert gas fusion technique.

These instruments feature our Cornerstone brand ® software, a custom interface designed specifically for

touch-screen operation. Developed by combining longterm research with customer feedback, this easy-to-use

software gives you complete access to instrument control, analysis settings, diagnostics, reporting, and more—without sacrificing valuable bench space.

全自动分析系统（可选） 。浙江LECO氧氮氢分析仪采购

Procedure - Solid Samples：

--Instrument calibration/drift correction.

Place the nickel basket containing the calibration/drift standard into the open port at the top of the loading head.

Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.

Clean the upper and lower electrode manually, or, if applicable, remove the crucible and press the analyze button to clean with the automatic cleaner.

氧氮氢分析仪的原理：分析样品在惰性气流存在下于石墨坩埚中加热熔融，其中脉冲炉温度可自由设定，并通过一个非接触式的光学温度传感器进行实时监控，用于实现样品的完全分解，反应所生成的CO H2和N2被带入到具有高稳定性和灵敏度的检测系统进行检测。对于CO的检测采用的是非色散性红外检测器，对于N2和H2的检测则采用热导检测器。

氧氮氢分析仪的特点：快速准确分析，自动化操作；精密气体校准；CO红外检测器，高分辨率和重现性的N、H热导池检测器；同一台仪器实现熔融提取和热提取；热提取分析时间可调；可自由选择温度*高达2500 °C；光学温度计温度测定和控制；所有检测器自动调零/自动水平控制（ALC）；数据评估的自动优化选择范围；炉自动清洁和坩埚自动进样（可选）；外设电脑进行操作和控制；样品信息保存； 所有样品数据可追踪查询；通过FTP或本地局域网进行数据传输； ON，H分析轻松切换。

Procedure – Powder/Chip Samples

Instrument calibration/drift correction.

Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.

Place the Nickel Capsule containing the sample into the open port at the top of the loading head.

Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.

Clean the upper and lower electrode either manually or remove the crucible and press the analyze button to clean with an automatic cleaner if applicable.

Summary

The determination of the amount of oxygen, nitrogen, and hydrogen in iron, steel, nickel-, and cobalt-base alloys represents some of the most important quality metrics for these materials. Oxygen is used to create steel from pig iron by removing excess carbon. Oxygen content must be controlled to limit the amount of carbon monoxide that can be formed during solidification which may cause excessive porosity. Nitrogen is considered both an impurity as well as an important alloying agent. Itcan be present as a nitride or interstitially in its gaseous form. Increased nitrogen content is known to increase yield and tensile strength, thus decreasing ductility and formability. Excessive levels may evolve during solidification thus increasing porosity. High hydrogen content is the primary cause of embrittlement, blistering and flaking due to its high

mobility through the lattice and provides no potential alloying benefits. The ONH836 utilizes a high-power

electrode furnace to quickly and efficiently release the target gases from within the sample, which allows

for a very rapid simultaneous determination of oxygen, nitrogen, and hydrogen.

减少了繁琐的额外数据处理。山西氧氮氢分析仪多少钱

Cornerstone氧氮氢分析软件分成4个主要部分：分析、诊断、设定、仪器，界面可快速导航和组织。浙江LECO氧氮氢分析仪采购

氧氮氢分析仪的常见故障及解决方法：

氧和氮空白值超过20。这是由于气流小，不能将炉子中的空气驱赶出去。可调节气体流量，调节载气压力在0.2~0.4MPa。接通仪器载气，放一个石墨坩埚在下电极上，打开主电源开关，点击软件上的关炉按钮，关闭炉子并等待10s。调节流量调节器，直到流量计a显示为30L／h，打开炉子。调节调节器直到流量计b显示为50L／h，再次关闭炉子。如果以上设置不稳定，则增加流量至100L／h，反复调节直至仪器稳定。 浙江LECO氧氮氢分析仪采购

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