Procedure – Powder/Chip Samples
Instrument calibration/drift correction.
Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.
Place the Nickel Capsule containing the sample into the open port at the top of the loading head.
Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.
Clean the upper and lower electrode either manually or remove the crucible and press the analyze button to clean with an automatic cleaner if applicable.
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Instrument calibration/drift correction.
a. Login a minimum of 3 Standard replicates.
b. Weigh a ~1.000 gram of a calibration/drift standard, enter the mass and standard identification into appropriate replicate fields.
c. Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.
d. Place the calibration/drift standard into the open port at the top of the loading head.
e. Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.
Sample Preparation
Sampling and sample preparation of refractory metals such as titanium and zirconium is somewhat different from that of steel. Unlike steel samples, hydrogen is not as mobile in this group of materials; therefore, storage in liquid nitrogen or dry ice is not required. However, it is important to keep the sample cool when cutting or sectioning. Sample preparation for oxygen and nitrogen determination has beendifferent from that of hydrogen determination.
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工具条、滑动条和下拉式菜单简化了校正和数据处理的参数设定。广东分析仪多少钱
Determine the instrument blank.
a. Login a minimum of 3 Blank replicates.
b. Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.
c. Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.
d. Clean the upper and lower electrode manually, or, if applicable, remove thecrucible and press the analyze button to clean with the automatic cleaner.
e. Firmly place a graphite crucible on the lower electrode tip.
f. Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and endautomatically.
g. Repeat steps 2b through 2f a minimum of three times.
h. Set the blank following the procedure outlined in the operator's instruction manual.
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