Procedure - Solid Samples
Instrument calibration/drift correction.
Add approximately 0.05 g of *** Graphite Powder to a *** Graphite Crucible.
Firmly place the crucible on the lower electrode tip or appropriate autoloader position.
Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically.
Repeat steps 3b through 3j a minimum of three times for each calibration/drift standard used.
Calibrate/drift following the procedure outlined in the operator's instruction manual.
Procedure – Powder/Chip Samples
Determine the instrument blank.
Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.
Clean the upper and lower electrode either manually or remove the crucible and press the analyze button to clean with an automatic cleaner if applicable.
Add approximately 0.05 g of *** Graphite Powder to a 782-720 Graphite Crucible.
Firmly place the crucible on the lower electrode tip or appropriate autoloader position.
Oxygen, Nitrogen, and Hydrogen in Refractory Metals
Summary
Titanium is a metal that can be combined with elements such as aluminum, vanadium, molybdenum, and tin to produce high-strength, lowdensity, and corrosion-resistant alloys. Titanium alloys are used by the military, medical devices, sporting goods, and aerospace industries because of these properties, and due to the strict demands of these industries, effort needs to be taken to assure that the material meets the highest of quality standards.
Summary
The determination of the amount of oxygen, nitrogen, and hydrogen in iron, steel, nickel-, and cobalt-base alloys represents some of the most important quality metrics for these materials. Oxygen is used to create steel from pig iron by removing excess carbon. Oxygen content must be controlled to limit the amount of carbon monoxide that can be formed during solidification which may cause excessive porosity. Nitrogen is considered both an impurity as well as an important alloying agent. Itcan be present as a nitride or interstitially in its gaseous form. Increased nitrogen content is known to increase yield and tensile strength, thus decreasing ductility and formability. Excessive levels may evolve during solidification thus increasing porosity. High hydrogen content is the primary cause of embrittlement, blistering and flaking due to its high
mobility through the lattice and provides no potential alloying benefits. The ONH836 utilizes a high-power
electrode furnace to quickly and efficiently release the target gases from within the sample, which allows
for a very rapid simultaneous determination of oxygen, nitrogen, and hydrogen.
双直流风扇保证持续冷却，不受电压波动的影响。
Sample Preparation
Typically, titanium and zirconium samples are chemically etched to remove surface contamination when oxygen and nitrogen are determined. However, etching can introduce hydrogen into the sample.
ASTM method E 1409 "Determination of Oxygen and Nitrogen in Titanium and Titanium Alloys by the Inert
Gas Fusion Technique", as updated in 1996, permits either etching or abrading (filing) of the test specimen.
ASTM E 1447 "Determination of Hydrogen in Titanium and Titanium Alloys by the Inert Gas Fusion Thermal
Conductivity/Infrared Detection Method" permits surface preparation by abrading (if necessary to remove
contamination). Differences in sample preparation present somewhat of a dilemma regarding simultaneous
determination of O, N, and H in titanium. However, abrading samples with a file to remove surface
contamination will yield accurate O, N, and H results. The ONH836 utilizes a high-power electrode furnace to quickly and efficiently release the target gases from within the sample, which allows for a very rapid simultaneous determination of oxygen, nitrogen, and hydrogen.
高速全自动真空除尘装置直接将粉尘排至仪器外部捕集器中，消除环境污染。浙江元素分析仪采购**的动态流量补偿（DFC）保证热导池气体流量、压力恒定。江苏专业元素分析仪哪家好
力可ONH836氧氮氢分析仪
特点和优势
国际**的非色散红外及热导检测器 ，无移动部件，不需要手动调整
采用三个**的红外器检测氧含量，同时检测CO和CO2，然后在转化为CO2集中检测，原理上是**完善的，所以不仅可以保证中间量程的测量精度，在**含量和高含量的检测范围内同样可以满足精度要求
高性能的红外检测器配置***恒温绝热技术，消除了外界环境温度的干扰
长寿命的红外发射光源和无漂移的电路设计保证检测器的长期稳定性
力可**的动态流量补偿控制DFC系统，保证了流量系统的完善，可以精确控制整个气路中的流量，保持流量恒定**改善了材料中氮分析的准确度
可以旁路的OMI-2 气路强化过滤装置增强了检测器的稳定性，使得分析结果更加准确
可选自动功能
20位试样自动进样系统
通用下电极坩埚支座，容纳各种坩埚使用
无需人工干预的全自动清扫系统
江苏专业元素分析仪哪家好
上海禹重实业有限公司位于友东路237号1幢104室。禹重科技致力于为客户提供良好的光谱仪，色谱仪，质谱仪，样品前处理，一切以用户需求为中心，深受广大客户的欢迎。公司注重以质量为中心，以服务为理念，秉持诚信为本的理念，打造仪器仪表良好品牌。在社会各界的鼎力支持下，持续创新，不断铸造***服务体验，为客户成功提供坚实有力的支持。
