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Procedure – Powder/Chip Samples

Determine the instrument blank.

Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically.

Repeat steps 2b through 2g a minimum of three times.

Set the blank following the procedure outlined in the operator's instruction manual.

Instrument calibration/drift correction.

Login a minimum of three Standard reps.

Weigh approximately *** grams of a calibration/drift standard into a *** Nickel Capsule; enter the mass and standard identification into appropriate rep fields. If applicable, place the nickel capsule in the appropriate autoloader position.

Note: LECO Reference Materia***o not require preparation. See preparation statement on the reference material certificate. Solid Standards may be used to calibrate when chip or powder standards are not available.

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力可OHN736&836系列仪器采用惰性熔融法，提供各种无机材料、钢铁、有色金属、硬质合金陶瓷材料中宽范围的氧氮氢同时测定。ONH836仪器通过***采纳客户的反馈意见和创新设计，力可***仪器采用触摸屏技术和在线软件平台，增强了仪器的可操作性，降低了分析成本，节省实验室桌面空间。

用户友好界面的Cornerstone™ 软件

力可**的Cornerstone碳硫分析软件采用触摸屏界面使用户可完整的达到分析控制、方法设定、在线诊断、数据报告。Cornerstone碳硫分析软件允许用户在单一分析界面中完成日常的所有工作，快速而且简单易用。力可创新的批次和重复样品数据分组功能极大简化了样品结果输出和结果标准偏差的自动计算。减少了繁琐的额外数据处理。

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氧氮氢分析仪的优点

采用惰气熔融技术，同时测定氧、氮和氢元素含量

新设计封闭气路系统，优化气路循环，使氧氮氢测量更准确

可采用更廉价的氩气作为载气

催化炉温度可调，使氧的测量更加准确

气路系统都采用电磁阀控制，新增分段式漏气检测

水冷样品加样端口，有效隔绝杂质气体侵入

仪器配置和氧、氮、氢测量范围可灵活选择

新设计的高灵敏度红外检测池和热导池，有极低的检出限

分析时间短

脉冲炉功率高达8.5kw，温度3000℃

颗粒状样品无需胶囊包裹，使用经济实惠

化学试剂及管路隐藏在门后（可移除）

强大的分析软件（支持数据和应用报告导出、增加评论区及其他更多功能）。

单点和多点校正（线性回归）

可采用自来水、冷却循环水机或交换机冷却

新设计的产品可用于各类生产控制和实验室。

company profile

Shanghai Uzong Industrial Co., Ltd. (hereinafter referred to as UZONGLAB®) is a high-tech company that provides integrated solutions for intelligent laboratories, mainly serving the Chinese market and countries along the “Belt and Road”. It has three business divisions and one The technology center, namely the instrument business department, consumables business department, project development department, and Zhongyu Lianhe Technology Center. In addition to the Shanghai headquarters, we have established branches in Beijing, Shenyang, Shijiazhuang, Taiyuan, Qingdao, Guangzhou, Chengdu and Urumqi. To provide customers with more professional, safer and more convenient products and services is our sole goal. 氧高低双量程采用3个碳红外检测一氧化碳和二氧化碳，保证准确定量。

Oxygen, Nitrogen, and Hydrogen in Refractory Metals

Summary

One of the most critical chemical specifications of titanium alloys is the hydrogen content. Too high of a

hydrogen content can cause hydrides to precipitate, which can lead to embrittlement and subsequent

cracking when the alloy is stressed. Hydrogen pickup typically occurs during downstream processing steps

such as heat treating, pickling, and cleaning.

The LECO ONH836 is a simultaneous oxygen, nitrogen, and hydrogen determinator that utilizes an electrode furnace, inert carrier gas, and both infrared and thermal conductivity detection to meet the analytical needs of the refractory metal industry. 

This application note was written specifically for use with the LECO ONH836 series determinator.

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