Procedure – Powder/Chip Samples
Instrument calibration/drift correction.
Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.
Place the Nickel Capsule containing the sample into the open port at the top of the loading head.
Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.
Clean the upper and lower electrode either manually or remove the crucible and press the analyze button to clean with an automatic cleaner if applicable.
美国LECO力可氧氮氢分析仪ONH836(氧氮氢联测仪)系列硬件部分
特点和优势
1、炉头区域LED照明系统
2、炉头快速拆装的粉尘过滤装置
3、装有自动旁路阀的可快速拆装氧水捕集装置
4、**的动态流量补偿(DFC)保证热导池气体流量、压力恒定
5、改进的红外检测池技术
新红外池的恒温绝热技术消除了外界环境温度的干扰
长寿命的红外发射光源和无漂移的电路设计保证红外检测池的长期稳定
氧高低双量程采用3个碳红外检测器,同时检测一氧化碳和二氧化碳,保证准确定量
6、高效脉冲炉冷却系统
强力内循环水冷装置
双直流风扇保证持续冷却,不受电压波动的影响
新电极炉头设计,提高脉冲炉热交换效率
7、全自动分析系统(可选)
自动清扫装置
20位或100位全自动分析系统
高速全自动真空除尘装置直接将粉尘排至仪器外部捕集器中,消除环境污染
浙江美国LECO氧氮氢分析仪厂家直销提供各种无机材料、钢铁、有色金属、硬质合金陶瓷材料中宽范围的氧氮氢同时测定。
Sample Preparation
Sampling and sample preparation is an important issue because traditional methods used to obtain samples for oxygen and nitrogen determination are different from those recommended for hydrogen, especially when sampling molten metal. The main difference in steel sampling procedures for oxygen/nitrogen and hydrogen is due to the mobilityof hydrogen. Special precautions must be used when sampling for hydrogen. From molten steel and iron, a sample must be quickly quenched in cold water and chilled in a refrigerant such as liquefied nitrogen or a mixture of acetone and solid carbon dioxide in order to reduce losses of hydrogen from diffusion. Losses of oxygen and nitrogen from diffusion are not a problem. A sample that is taken for hydrogen and
chilled in a refrigerant can also be used for oxygen and nitrogen determination. However, a sample that is typically taken for oxygen and/or nitrogen determination is not suitable for hydrogen determination due to hydrogen loss (diffusion). Surface contamination must be removed by filing or light grinding, using care not to overheat the sample.
Method Selection
Two methods are described in this application note; either method can be used to analyze iron, steel, nickel-, and cobalt-base alloys. The Precision Method is recommended for general use and will provide the best precision and accuracy throughout the typical O, N, and H concentrations found in this group of metals; approximate cycle time is 3.5 minutes. The Fast Track method can be used where speed of analysis is a critical component; for example, when molten metal is being sampled and results are required in the shortest possible time. This method will produce suitable results for most samples; approximate cycle time is 2.25 minutes. As noted above, sampling and sample preparation are key elements to accurate O, N, and Hdetermination as well. It is up to the user to determine which method best meets their needs.
试样加载过程中完全密闭,消除大气的中可能带来的杂质的污染。
Instrument Highlights and Features
Features and Benefits
LED light ring illuminates the furnace area
Choice of either argon or helium carrier gas
Novel electrode design increases heat transfer efficiency for increased stability
Non-touch interface systems are also available
User-friendly brand software
High-Performance Detector Design
Thermostatic construction provides increased protection from ambient temperature fluctuations
Optimized emitter control and detection circuitryimproves the IR cell lifetime and long-term stability,
resulting in superior accuracy and precision
Infrared detection for the determination of oxygen, thermoconductivity detection for the determination
of nitrogen
**的动态流量补偿(DFC)保证热导池气体流量、压力恒定。江苏美国分析仪价格
高速全自动真空除尘装置直接将粉尘排至仪器外部捕集器中,消除环境污染。浙江美国LECO氧氮氢分析仪厂家直销
Instrument Highlights and Features
Optional Features
Optional boom-mounted touch-screen interface package (M) promotes an ergonomic workspace
Optional Performance Package (P) adds a three-stage carrier gas purification system, and a dual-loop gas dose module
Optional Dual Cooling Package (D) adds an integratedliquid-to-air radiator with dual cooling fans. This DC
option gives the user the choice of liquid-to-liquid cooling, liquid-to-air cooling, or a combination of both
Optional integrated autocleaner (H) automatically cleans the upper electrode and lower electrode tip
Optional 20-sample shuttle loader available
浙江美国LECO氧氮氢分析仪厂家直销
液压万能试验机的油泵调试以及试验步骤:1、接好电源线,按“电源”按钮,指示灯亮。2、根据试样规格选择...
【详情】在这些领域中流量计主要是取到检查和测量的作用。能源计量。煤炭、原油、煤层气、石油气天然气等一次能源,...
【详情】现在,质量流量计在质量流量测试仪中处于主导地位,相信一直以这种理念发展下去的话,在这个行业中一直保持...
【详情】万能试验机人们往往将数据的稳定显示看的非常重要,而忽略了数据的真实性,将滤波器的截止频率设置的非常低...
【详情】万能试验机安装在清洁干燥而且温度均匀的房屋内同时应考虑到在机器上作较长的长梁弯曲试验的可能性以及使用...
【详情】电液伺服万能试验机集电液伺服自动控制、自动测量、数据采集、屏幕显示、试验结果处理为一体,以油缸下置式...
【详情】