Determine the instrument blank.
a. Login a minimum of 3 Blank replicates.
b. Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open.
c. Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.
d. Clean the upper and lower electrode manually, or, if applicable, remove thecrucible and press the analyze button to clean with the automatic cleaner.
e. Firmly place a graphite crucible on the lower electrode tip.
f. Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and endautomatically.
g. Repeat steps 2b through 2f a minimum of three times.
h. Set the blank following the procedure outlined in the operator's instruction manual.
新型气路管道减少气路连接阀,使得漏气,断路故障更少。北京分析仪多少钱
Method Selection
Two methods are described in this application note; either method can be used to analyze iron, steel, nickel-, and cobalt-base alloys. The Precision Method is recommended for general use and will provide the best precision and accuracy throughout the typical O, N, and H concentrations found in this group of metals; approximate cycle time is 3.5 minutes. The Fast Track method can be used where speed of analysis is a critical component; for example, when molten metal is being sampled and results are required in the shortest possible time. This method will produce suitable results for most samples; approximate cycle time is 2.25 minutes. As noted above, sampling and sample preparation are key elements to accurate O, N, and Hdetermination as well. It is up to the user to determine which method best meets their needs.
山西美国分析仪简化日常分析所需的炉头进样部分机械维护工作。
Oxygen, Nitrogen, and Hydrogen in Refractory Metals
Summary
One of the most critical chemical specifications of titanium alloys is the hydrogen content. Too high of a
hydrogen content can cause hydrides to precipitate, which can lead to embrittlement and subsequent
cracking when the alloy is stressed. Hydrogen pickup typically occurs during downstream processing steps
such as heat treating, pickling, and cleaning.
The LECO ONH836 is a simultaneous oxygen, nitrogen, and hydrogen determinator that utilizes an electrode furnace, inert carrier gas, and both infrared and thermal conductivity detection to meet the analytical needs of the refractory metal industry.
This application note was written specifically for use with the LECO ONH836 series determinator.
Procedure – Powder/Chip Samples
Prepare the instrument as outlined in the operator's instruction manual.
Login a minimum of three Blank reps.
Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open. Insert a *** Nickel Capsule (leave capsule open) into the open port at top of loading head.
Note: samples using automation should be placed in the appropriate autoloader position before starting the analysis sequence. Once the sequence has started, the automatic analysis will start and end automatically.
Procedure – Powder/Chip Samples
Instrument calibration/drift correction.
Calibrate/drift following the procedure outlined in the operator's instruction manual.
Login Sample with the appropriate number of reps.
Weigh approximately *** grams of appropriately prepared sample into a *** Nickel Capsule, enter mass and sample identification into appropriate rep fields. If applicable, place the nickel capsule in the
appropriate autoloader position.
Repeat steps 3c through 3i for sample analysis.
Cornerstone氧氮氢分析软件分成4个主要部分:分析、诊断、设定、仪器,界面可快速导航和组织。北京分析仪多少钱
美国LECO力可氧氮氢分析仪ONH836(氧氮氢联测仪)系列硬件部分
特点和优势
1、炉头区域LED照明系统
2、炉头快速拆装的粉尘过滤装置
3、装有自动旁路阀的可快速拆装氧水捕集装置
4、**的动态流量补偿(DFC)保证热导池气体流量、压力恒定
5、改进的红外检测池技术
新红外池的恒温绝热技术消除了外界环境温度的干扰
长寿命的红外发射光源和无漂移的电路设计保证红外检测池的长期稳定
氧高低双量程采用3个碳红外检测器,同时检测一氧化碳和二氧化碳,保证准确定量
6、高效脉冲炉冷却系统
强力内循环水冷装置
双直流风扇保证持续冷却,不受电压波动的影响
新电极炉头设计,提高脉冲炉热交换效率
7、全自动分析系统(可选)
自动清扫装置
20位或100位全自动分析系统
高速全自动真空除尘装置直接将粉尘排至仪器外部捕集器中,消除环境污染
北京分析仪多少钱
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