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Oxygen, Nitrogen, and Hydrogen in Refractory Metals

Summary

One of the most critical chemical specifications of titanium alloys is the hydrogen content. Too high of a

hydrogen content can cause hydrides to precipitate, which can lead to embrittlement and subsequent

cracking when the alloy is stressed. Hydrogen pickup typically occurs during downstream processing steps

such as heat treating, pickling, and cleaning.

The LECO ONH836 is a simultaneous oxygen, nitrogen, and hydrogen determinator that utilizes an electrode furnace, inert carrier gas, and both infrared and thermal conductivity detection to meet the analytical needs of the refractory metal industry. 

This application note was written specifically for use with the LECO ONH836 series determinator.


采用三个**的红外器检测氧含量,同时检测CO和CO2,然后在转化为CO2集中检测。山西LECO氧氮氢分析仪价格

ONH836系列:氧氮氢分析仪(熔融法)

软件特点和优势

Cornerstone氧氮氢分析软件分成4个主要部分:分析、诊断、设定、仪器,界面可以快速导航和组织。工具条、滑动条和下拉式菜单简化了校正和数据处理的参数设定。分析软件同时包括实时的环境参数的监测,提供完整的系统图表模拟。高级诊断程序包括全数字化的在线操作手册、维护模拟演示、图片说明等提供快速指导。Cornerstone氧氮氢分析软件同时支持***的数据文档格式和可变的报告格式。 山东美国分析仪采购20位或100位全自动分析系统。

Procedure – Powder/Chip Samples

Instrument calibration/drift correction.

Calibrate/drift following the procedure outlined in the operator's instruction manual.


Analyze Samples.

Login Sample with the appropriate number of reps.

Weigh approximately *** grams of appropriately prepared sample into a *** Nickel Capsule, enter mass and sample identification into appropriate rep fields. If applicable, place the nickel capsule in the

appropriate autoloader position.

Repeat steps 3c through 3i for sample analysis.


Procedure – Powder/Chip Samples

Determine the instrument blank.


Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically.


Repeat steps 2b through 2g a minimum of three times.


Set the blank following the procedure outlined in the operator's instruction manual.


Instrument calibration/drift correction.

Login a minimum of three Standard reps.


Weigh approximately *** grams of a calibration/drift standard into a *** Nickel Capsule; enter the mass and standard identification into appropriate rep fields. If applicable, place the nickel capsule in the appropriate autoloader position.


Note: LECO Reference Materia***o not require preparation. See preparation statement on the reference material certificate. Solid Standards may be used to calibrate when chip or powder standards are not available.




长寿命的红外发射光源和无漂移的电路设计保证检测器的长期稳定性。

Procedure - Solid Samples

Prepare the instrument as outlined in the operator's instruction manual.


Determine the instrument blank.

Login a minimum of 3 Blank replicates.

Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open. Place a 502-344 Nickel Basket into the loading head.

Note: samples using automation should be placed in the appropriate autoloader position before starting the

analysis sequence. Once the sequence has started, the automatic analysis will start and end automatically.


氧氮氢分析仪怎么选?欢迎联系上海禹重科技,我司产品质量保证,欢迎咨询!山东美国分析仪采购

改进的红外检测池技术。山西LECO氧氮氢分析仪价格

736 Series: Oxygen/Nitrogen by Inert Gas Fusion


The 736 family of Elemental Analyzers is designed for routine measurement of oxygen and nitrogen content of

inorganic materials, ferrous and nonferrous alloys, andrefractory materials using the inert gas fusion technique.

These instruments feature our Cornerstone brand ® software, a custom interface designed specifically for

touch-screen operation. Developed by combining longterm research with customer feedback, this easy-to-use

software gives you complete access to instrument control, analysis settings, diagnostics, reporting, and more—without sacrificing valuable bench space.


山西LECO氧氮氢分析仪价格

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