Sample Preparation
Typically, titanium and zirconium samples are chemically etched to remove surface contamination when oxygen and nitrogen are determined. However, etching can introduce hydrogen into the sample.
ASTM method E 1409 "Determination of Oxygen and Nitrogen in Titanium and Titanium Alloys by the Inert
Gas Fusion Technique", as updated in 1996, permits either etching or abrading (filing) of the test specimen.
ASTM E 1447 "Determination of Hydrogen in Titanium and Titanium Alloys by the Inert Gas Fusion Thermal
Conductivity/Infrared Detection Method" permits surface preparation by abrading (if necessary to remove
contamination). Differences in sample preparation present somewhat of a dilemma regarding simultaneous
determination of O, N, and H in titanium. However, abrading samples with a file to remove surface
contamination will yield accurate O, N, and H results. The ONH836 utilizes a high-power electrode furnace to quickly and efficiently release the target gases from within the sample, which allows for a very rapid simultaneous determination of oxygen, nitrogen, and hydrogen.
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仪器启动时显示。没有水流。系统分析电流切断，分析停止。这是水流探测器不正常，水泵不工作，管道堵塞。将仪器的右面板取下，观察水流探测器，用手挤压补水塑料水瓶，发现水流正常，显示正常，证明水流探测器正常，管道畅通。启动循环水泵，但分析仪显示没有水流，此时可判定水泵不正常。打开水泵转子密封口，启动泵发现电机正常运转，此时关闭进水，拆下水泵，发现叶轮脱落。经了解，判定是由于外部冷却水停水，仪器内循环水温过高（水温应≤70℃），致使叶轮（叶轮材料PVC）热胀并脱轴。用粘合剂粘合叶轮后再粘于叶轮轴上，待粘合剂凝固后试车，仪器运行正常。 北京美国分析仪哪家好***红外池的恒温绝热技术消除了外界环境温度的干扰。
Instrument calibration/drift correction
f. Clean the upper and lower electrode manually, or, if applicable, remove the crucible and press the analyze button to clean with the automatic cleaner.
g. Firmly place a graphite crucible on the lower electrode tip.
h. Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically.
i. Repeat steps 3b through 3h a minimum of three times for each calibration/drift standard used.
. Calibrate/drift following the procedure outlined in the operator's instruction manual.
氧氮氢分析仪是快速、准确分析氧、氮、氢元素的、高性能仪器，整机采用模块化、一体化设计，即主机由可靠的脉冲电极炉、高灵敏高精度的检测系统、布局合理和气密性好的气路系统、可靠耐用的电源系统、稳定的电路系统、高校节能的水循环散热系统等六个**的硬件模块单元组成。
氧氮氢分析仪的测量原理：
测量范围非常***。分析样品时，样品被称重后放到样品端口中，然后用载气进行冲洗，防止大气（含氧气和氮气）进入到炉子系统中。
石墨坩埚在脉冲炉中脱气，以尽量减少自带的污染。经过稳定阶段后样品落入坩埚中并熔融。样品中的氧与石墨坩埚中的碳反应生成一氧化碳。氮和氢以单质的形式释放。载气和样品气体通过粉尘过滤网后再进入到氧化铜催化炉中，将一氧化碳氧化成二氧化碳。
二氧化碳进入到红外池中用于测定氧含量，被测后的气体导入化学试剂管，这时二氧化碳和水被化学试剂除去，氮元素通过热导检测池含量被测定。测量氢时，载气换为氮气，样品气体通过舒茨试剂而不是氧化铜催化剂。测氧和氮时也可采用更廉价的氩气作为载气。 国际**的非色散红外及热导检测器 ，无移动部件，不需要手动调整。
氧氮氢分析仪的常见故障及解决方法：
氧和氮空白值超过20。这是由于气流小，不能将炉子中的空气驱赶出去。可调节气体流量，调节载气压力在0.2~0.4MPa。接通仪器载气，放一个石墨坩埚在下电极上，打开主电源开关，点击软件上的关炉按钮，关闭炉子并等待10s。调节流量调节器，直到流量计a显示为30L／h，打开炉子。调节调节器直到流量计b显示为50L／h，再次关闭炉子。如果以上设置不稳定，则增加流量至100L／h，反复调节直至仪器稳定。 高性能的红外检测器配置***恒温绝热技术，消除了外界环境温度的干扰。山西进口分析仪厂家报价
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Instrument Highlights and Features
Optional Features
Optional boom-mounted touch-screen interface package (M) promotes an ergonomic workspace
Optional Performance Package (P) adds a three-stage carrier gas purification system, and a dual-loop gas dose module
Optional Dual Cooling Package (D) adds an integratedliquid-to-air radiator with dual cooling fans. This DC
option gives the user the choice of liquid-to-liquid cooling, liquid-to-air cooling, or a combination of both
Optional integrated autocleaner (H) automatically cleans the upper electrode and lower electrode tip
Optional 20-sample shuttle loader available
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